Synthesis and characterization of new stationary phases

- Synthesis of stationary phases in a capillary (by in situ polymerization of monoliths) to develop separation methods in HILIC mode for nanoLC

  • Collaborations: CEA
  • Fundings: DIM Analytics
  • Post-Doc : N. Henry (2013-2014)



- Insertion of stationary phases inside micro channels for GC on chip

Two ways are explored :

  • Sputtering
  • In situ synthesis of inorganic monoliths
  • Publications :
    • Sputtered silica, J. Vial et al. J. Chromatogr. A , 1214, 2011, 3262-326
    • Sputtered alumina, R. Haudebourg et al., Anal Bioanal Chem, 2014, 406,1245 – 1247
    • Review on stationnary phases, I.Azzouz et al. Anal Bioanal Chem, 2014, 406, 981 – 994

- Synthesis of selective stationary phases: immunosorbent, oligosorbent, MIP and stationary phases inducing a molecular recognition mechanism for the trace analysis :

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Practical information

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